A sulfur deprivation test was conducted in a sealed 250 ml vessel. More hydrogen was generated in this process than was anticipated, and the vessel cracked.
An incident occurred when Ti-doped sodium alanate was exposed to air, apparently resulting in an unstable compound that experienced a rapid exothermic reaction.
A researcher was working with hydrogen storage materials in a laboratory. Several other researchers were working in adjacent laboratories.
A fire erupted from a tanker truck delivering liquid hydrogen to a factory. The ignition of leaking vapors created a plume of flames that rose dozens of feet into the air. The flames receded within seconds, leaving the truck with little damage and its driver unharmed.
The truck was off-loading hydrogen into a tank behind the plant when the incident occurred. The plant reported no delays in its production. It uses the hydrogen in various processes.
A hydrogen cylinder was initially located in an adjacent laboratory, with tubing going through the wall into the laboratory in use. When the cylinder was moved to the laboratory in use, a required leak check was not performed. Unfortunately, a leak had developed that was sufficient to cause an accumulation of hydrogen to a level above the Lower Flammability Limit. The hydrogen ignited when a computer power plug was pulled from an outlet. The exact configuration of the leak location and the outlet plug is unknown.
A liquid hydrogen tank’s rupture disc failed prematurely, which caused the tank to vent its entire gas contents through the tank’s vent stack. Venting was very loud and formed a condensed moisture cloud visible from the top of the stack. Liquid air was also visible coming off the stack. Venting ceased after approximately 5 minutes. On-site staff called the fire department, which arrived promptly and evacuated the area. Normal operations resumed after the Fire Department was able to determine there were no unsafe conditions.
A facility uses small crucibles to heat precious metals within a fume hood, with natural gas as the fuel source for the Bunsen burner. Hydrogen is fed into the crucible at low pressure (<20 psi) to control the atmosphere within the vessel in order to prevent oxidation. The hydrogen is routed through a manifold with flexible tubing, which is connected to a ceramic tip and fitted into the crucible through a small opening in the crucible's lid. The hydrogen is consumed in the process. The facility believes that the hydrogen tubing developed a leak which eventually ignited.
A laboratory had an incident with an ammonia tank. When the valve was opened, the packing in the valve apparently "moved," and a faint ammonia smell was noticed. The tank was returned to the supplier.
While refilling the hydrogen system after an outage caused by a power failure, the excess flow valve located at the hydrogen tank tripped, but did not go fully shut.
A hydrogen gas detector on the ground floor of a building registered the release of a small amount of hydrogen gas and actuated automatic alarms both at the fire department and in one of its buildings. Additionally, interlocks connected to the gas detector completely shut down the experiment. Upon hearing the alarm, all occupants (about 6) promptly left the building. Fire department personnel are housed in the trailer next to a building and responded within one minute. They tested the atmosphere within the building, reset the gas detector, and secured the alarm at 9:15.