Gas Cylinder Inadvertently Replaced with Hydrogen Gas Cylinder for Use in AL Proportional Counter

First Name
Andy
Last Name
Piatt

A health physics technician (HPT) discovered that a scaler in an analytical laboratory was out of P-10 gas (90%Ar and 10% CH4). The HPT went to the building where auxiliary gas cylinders are stored. He located a P-10 gas cylinder and turned to search for a hand-cart. There were no hand-carts present, and the technician had to get one from another room. When he returned to the cylinder storage area, he loaded the wrong cylinder. It contained hydrogen gas instead, however, the two cylinders were next to each other and they were basically identical.

Small Glass Ampoule of Aluminum Hydride (Alane) Ruptures After Transit

First Name
Andy
Last Name
Piatt

A small research sample of approximately 5 grams of aluminum hydride (alane) doped with 2-3 mol % TiCl3 contained within a glass ampoule ruptured after transit while stored in an office cabinet. The rupture was attributed to over-pressurization caused by hydrogen gas buildup within the sample over a four-month period. The glass ampoule, contained within a 0.2-inch thick cardboard shipping tube, was not a pressure-rated container. The rupture resulted in glass chards penetrating the protective cardboard shipping tube.

Small Glass Vial of Aluminum Hydride Compound Ruptures in Glove Box

First Name
Andy
Last Name
Piatt

A closed 20-mL glass scintillation vial containing approximately 5 grams of an aluminum hydride compound ruptured and shattered, likely due to pressure buildup after 6 weeks of storage. The glass vial with aluminum hydride compound was stored inside a closed plastic box. The plastic box with vial was stored within an air-free glove box at room temperature. When the glass vial ruptured, the vial was contained within the plastic box; however, the plastic box door was forced slightly ajar. The ruptured containers and internal materials were fully contained within the glove box.

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