A large, hydrogen-cooled generator is driven by steam turbines at a power station. During maintenance shutdowns, the hydrogen cooling loop in the generator is purged with carbon dioxide. After CO2 concentrations are measured with a densitometer to verify the complete removal of hydrogen, the generator is purged with air and the maintenance is performed.

This purging procedure was used prior to the explosion. The CO2 reading was reported to be 100 percent CO2 at the top of the generator. The cooling system was then purged with air and a 1/2 inch pipe in the cooling loop was cut to install some new instrumentation. When the pipe was cut, pressurized gas was emitted at the opening. Workers assumed the gas was either carbon dioxide or air and proceeded with the new instrument view more

During preparation of a new hydrogen storage material, ammonia borane (AB) loaded onto mesoporous carbon, an unexpected incident was observed. As with all procedures with new materials the work is conducted on a small scale and in a laboratory fume hood. They followed the procedures that they had used for absorption of ammonia borane onto mesoporous silica without incident.

To absorb the solid AB into a scaffold material they dissolve AB in a dry aprotic polar solvent, THF. The saturated solution of AB in THF is added to the mesoporous carbon material in a round bottom flask, stirred for 10 minutes to saturate the mesoporous scaffold with AB and then the solvent is slowly removed under vacuum. At this point the sample is assumed to be prepared and ready for transfer to a sample view more